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Hierarchical structures of stainless steel 316L manufactured by Electron Beam Melting
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
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2017 (English)In: Additive Manufacturing, ISSN 2214-8604, E-ISSN 2214-7810, Vol. 17, p. 106-112Article in journal (Refereed) Published
Abstract [en]

One of the serious obstacles preventing wide industrial use of additive manufacturing (AM) in metals and alloys is a lack of materials available for this technology. It is particularly true for the Electron Beam Melting (EBM®) process, where only a few materials are commercially available, which significantly limits the use of the method. One of the dominant trends in AM today is developing processes for technological materials already widely used by other methods and developed for other industrial applications, gaining further advantages through the unique value added by additive manufacturing. Developing new materials specifically for additive manufacturing that can utilize the properties and specifics of the method in full is still a research and development subject, and such materials are yet far from full scale industrial usage. Stainless steels are widely used in industry due to good mechanical properties, corrosion resistance and low cost of material. Hence, there is potentially a market for this material and one possible business driver compared with casting for example is that lead times could be cut drastically by utilizing an additive approach for one-off or small series production. This paper presents results from the additive manufacturing of components from the known alloy 316L using EBM®. Previously the samples of 316L were made by laser-based AM technology. This work was performed as a part of the large project with the long term aim to use additively manufactured components in a nuclear fusion reactor. Components and test samples successfully made from 316L stainless steel using EBM® process show promising mechanical properties, density and hardness compared to its counterpart made by powder metallurgy (hot isostatic pressing, HIP). As with the other materials made by EBM® process, 316L samples show rather low porosity. Present paper also reports on the hierarchical microstructure features of the 316L material processed by EBM® characterized by optical and electron microscopy.

Place, publisher, year, edition, pages
2017. Vol. 17, p. 106-112
Keywords [en]
Electron beam melting, Stainless steel, 316L, Characterization, Microstructures
National Category
Materials Chemistry
Research subject
Materials Chemistry
Identifiers
URN: urn:nbn:se:su:diva-176454DOI: 10.1016/j.addma.2017.07.003ISI: 000457239900010Scopus ID: 2-s2.0-85028544889OAI: oai:DiVA.org:su-176454DiVA, id: diva2:1375882
Available from: 2019-12-06 Created: 2019-12-06 Last updated: 2022-03-25Bibliographically approved
In thesis
1. Additive metallurgy - Thermal influences on structure and properties of stainless steel 316L
Open this publication in new window or tab >>Additive metallurgy - Thermal influences on structure and properties of stainless steel 316L
2020 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Additive manufacturing (AM) as a manufacturing process has, in recent years, become widely accepted as capable of manufacturing parts that will be used in end products. In this thesis, stainless steel grade 316L parts are manufactured using two different powder bed fusion techniques, selective laser melting (SLM) and electron beam melting (EBM). It is recognized that parts made using these processes will have unique microstructures and mechanical properties that have not been seen in bulk parts produced with other methods. The driving force behind the formation of these structures is the fast cooling speed that induces segregation of elements, forming an inhomogeneous microstructure. How these structures react to thermal treatment is less well known and an essential aspect in many applications. Parts manufactured using SLM was treated with hot isostatic pressing (HIP) to investigate if the material retains its unique features. Two different HIP cycles were used, one with 1150 °C and one with 1040 °C. In both cases, the cellular sub-grain structure fades. The cycle utilizing the high temperature is found to coarsen the grain structure and thus lowering the mechanical properties significantly. As manufactured parts show yield strength (615±1 MPa), tensile strength (725±2 MPa) and microhardness (211±10 Hv), compared to values of yield strength (284±2 MPa), tensile strength (636±1 MPa) and microhardness (178±8 Hv) after 1150 °C HIP. Using HIP at 1040 °C, the material will retain a finer grain structure resulting in higher yield strength (417±7 MPa) compared to 1150 °C HIP temperature, while the UTS and hardness have a similar value. It is also observed that the dispersed inclusions formed during SLM are still present after HIP to increase the mechanical properties compared to a conventionally annealed bar (TS: 515 MPa, YS: 205 MPa). Samples manufactured using EBM was investigated to understand the influence of the in-situ heat treatment that is present in the EBM process. The material possesses a long-range heterogeneous structure in addition to the cellular structure, where the cellular structure is present at the top and disappears further down the sample. Samples with different geometries were produced to study the effect of heat flux, cooling speed and the elevated temperature of 800 °C that is present during the EBM process. The thickness of the cell boundaries is measured in different areas, revealing that geometry and size of manufactured parts have a significant impact on the evolving microstructure. It is also revealed that the tensile strength (562±4 MPa) and microhardness (161±11 Hv) is not affected by the change in microstructure, resulting in a very homogeneous material concerning these parameters. Heat treating the material at 800 °C show that the cellular structure becomes diffuse after several hours, but the grain morphology stays the same.

Place, publisher, year, edition, pages
Stockholm: Department of Materials and Environmental Chemistry, Stockholm University, 2020
Keywords
Additive manufacturing, Selective laser melting, Electron beam melting, Hot isostatic pressing, Stainless steel, Microstructural heterogeneity
National Category
Materials Chemistry
Research subject
Materials Chemistry
Identifiers
urn:nbn:se:su:diva-176458 (URN)978-91-7797-968-5 (ISBN)978-91-7797-969-2 (ISBN)
Public defence
2020-02-07, Magnélisalen, Kemiska övningslaboratoriet, Svante Arrhenius väg 16 B, Stockholm, 09:00 (English)
Opponent
Supervisors
Note

At the time of the doctoral defense, the following papers were unpublished and had a status as follows: Paper 5: Manuscript. Paper 6: Manuscript.

Available from: 2020-01-15 Created: 2019-12-09 Last updated: 2022-02-26Bibliographically approved

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Olsén, JonSaeidi, KamranShen, Zhijian

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