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Determination of benzothiazole and benzotriazole derivates in tire and clothing textile samples by high performance liquid chromatography-electrospray ionization tandem mass spectrometry
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för analytisk kemi.
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för analytisk kemi.ORCID-id: 0000-0002-1598-7093
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för analytisk kemi.
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för analytisk kemi.
Vise andre og tillknytning
2013 (engelsk)Inngår i: Journal of Chromatography A, ISSN 0021-9673, E-ISSN 1873-3778, Vol. 1307, s. 119-125Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

A high performance liquid chromatography–tandem mass spectrometry method utilizing electrospray ionization in positive and negative mode has been developed for the separation and detection of benzothiazole and benzotriazole derivates. Ultra-sonication assisted solvent extraction of these compounds has also been developed and the overall method demonstrated on a selected clothing textile and an automobile tire sample. Matrix effects and extraction recoveries, as well as linearity and limits of detection have been evaluated. The calibration curves spanned over more than two orders of magnitude with coefficients of correlation R2 > 0.99 and the limits of detection and the limits of quantification were in the range 1.7–58 pg injected and 18–140 pg/g, respectively. The extraction recoveries ranged between 69% and 102% and the matrix effects between 75% and 101%. Benzothiazole and benzotriazole derivates were determined in the textile sample and benzothiazole derivatives determined in the tire sample with good analytical performance.

sted, utgiver, år, opplag, sider
2013. Vol. 1307, s. 119-125
Emneord [en]
HPLC–MS/MS, Benzothiazoles, Benzotriazoles, Automobile tire, Textile sample
HSV kategori
Identifikatorer
URN: urn:nbn:se:su:diva-93450DOI: 10.1016/j.chroma.2013.07.087ISI: 000324005500015OAI: oai:DiVA.org:su-93450DiVA, id: diva2:646948
Tilgjengelig fra: 2013-07-26 Laget: 2013-09-10 Sist oppdatert: 2019-12-09bibliografisk kontrollert

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Avagyan, RozannaSadiktsis, IoannisThorsen, GunnarÖstman, ConnyWesterholm, Roger
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