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Efficient DBU accelerated synthesis of F-18-labelled trifluoroacetamides
Stockholm University, Faculty of Science, Department of Organic Chemistry.ORCID iD: 0000-0002-1333-7740
Stockholm University, Faculty of Science, Department of Organic Chemistry.ORCID iD: 0000-0003-4299-8860
Stockholm University, Faculty of Science, Department of Organic Chemistry. Karolinska Institutet, Sweden.
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2016 (English)In: Chemical Communications, ISSN 1359-7345, E-ISSN 1364-548X, Vol. 52, no 97, p. 13963-13966Article in journal (Refereed) Published
Abstract [en]

Nucleophilic F-18-fluorination of bromodifluoromethyl derivatives was performed using [F-18] Bu4NF in the presence of DBU(1,8-diazabicyclo[5.4.0]undec-7-ene). This novel procedure provided a diverse set of [F-18] trifluoroacetamides in good to excellent radiochemical conversions. A mechanism where DBU acts as organomediator in this transformation is proposed.

Place, publisher, year, edition, pages
Royal Society of Chemistry, 2016. Vol. 52, no 97, p. 13963-13966
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Chemical Sciences
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URN: urn:nbn:se:su:diva-139349DOI: 10.1039/c6cc08535kISI: 000390436700005PubMedID: 27844069OAI: oai:DiVA.org:su-139349DiVA, id: diva2:1072378
Funder
Swedish Research CouncilKnut and Alice Wallenberg FoundationAvailable from: 2017-02-07 Created: 2017-02-06 Last updated: 2019-05-08Bibliographically approved

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Bermejo Gómez, AntonioCortes, Miguel AngelLübcke, MarvinSzabó, Kálmán J.
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