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Chemoenzymatic Dynamic Kinetic Resolution of Secondary Alcohols Using an Air- and Moisture-Stable Iron Racemization Catalyst
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Number of Authors: 4
2017 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 23, no 5, 1048-1051 p.Article in journal (Refereed) Published
Abstract [en]

Herein, we report on a metalloenzymatic dynamic kinetic resolution of sec-alcohols employing an iron-based racemization catalyst together with a lipase. The iron catalyst was evaluated in racemization and then used in dynamic kinetic resolution of a number of sec-alcohols to give enantiomerically pure products in good to high yields. The iron catalyst is air and moisture stable and is readily accessible.

Place, publisher, year, edition, pages
2017. Vol. 23, no 5, 1048-1051 p.
Keyword [en]
dynamic kinetic resolution, enzyme catalysis, iron catalysis, racemization, secondary alcohols
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-141286DOI: 10.1002/chem.201605754ISI: 000395753000014PubMedID: 28005307OAI: oai:DiVA.org:su-141286DiVA: diva2:1086882
Available from: 2017-04-04 Created: 2017-04-04 Last updated: 2017-04-04Bibliographically approved

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Gustafson, Karl P. J.Gudmundsson, ArnarBäckvall, Jan-E.
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