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Mild Reductive Functionalization of Amides into N-Sulfonylformamidines
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.ORCID iD: 0000-0003-2013-8093
Stockholm University, Faculty of Science, Department of Organic Chemistry.ORCID iD: 0000-0003-1271-4601
Stockholm University, Faculty of Science, Department of Organic Chemistry. Umeå University, Sweden.ORCID iD: 0000-0001-5887-4630
2017 (English)In: ChemistryOpen, ISSN 2191-1363, Vol. 6, 484-487 p.Article in journal (Refereed) Published
Abstract [en]

The development of a protocol for the reductive functionalization of amides into N-sulfonylformamidines is reported. The one-pot procedure is based on a mild catalytic reduction of tertiary amides into the corresponding enamines by the use of Mo(CO)6 (molybdenum hexacarbonyl) and TMDS (1,1,3,3-tetramethyldisiloxane). The formed enamines were allowed to react with sulfonyl azides to give the target compounds in moderate to good yields.

Place, publisher, year, edition, pages
2017. Vol. 6, 484-487 p.
National Category
Organic Chemistry
Research subject
Organic Chemistry
Identifiers
URN: urn:nbn:se:su:diva-145556DOI: 10.1002/open.201700087ISI: 000407167100006OAI: oai:DiVA.org:su-145556DiVA: diva2:1130291
Available from: 2017-08-09 Created: 2017-08-09 Last updated: 2017-09-18Bibliographically approved
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