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A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).ORCID iD: 0000-0001-9118-1342
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Number of Authors: 82017 (English)In: Review of Scientific Instruments, ISSN 0034-6748, E-ISSN 1089-7623, Vol. 88, no 10, article id 104102Article in journal (Refereed) Published
Abstract [en]

A new versatile and easy-to-use remote-controlled reactor setup aimed at the analysis of chemical reactions under solvothermal conditions has been constructed. The reactor includes a heating system that can precisely control the temperature inside the reaction vessels in a range between ambient temperature and 180 degrees C. As reaction vessels, two sizes of commercially available borosilicate vessels (V-max = 5 and 11 ml) can be used. The setup furthermore includes the option of stirring and injecting of up to two liquid additives or one solid during the reaction to initiate very fast reactions, quench reactions, or alter chemical parameters. In addition to a detailed description of the general setup and its functionality, three examples of studies conducted using this setup are presented.

Place, publisher, year, edition, pages
2017. Vol. 88, no 10, article id 104102
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Other Engineering and Technologies Physical Sciences
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URN: urn:nbn:se:su:diva-149860DOI: 10.1063/1.4999688ISI: 000414174000030PubMedID: 29092509OAI: oai:DiVA.org:su-149860DiVA, id: diva2:1164713
Available from: 2017-12-11 Created: 2017-12-11 Last updated: 2018-08-31Bibliographically approved

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Inge, Andrew KentaroDippel, A. -C.
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