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Methods for trace analysis of short-, medium-, and long-chain chlorinated paraffins: Critical review and recommendations
Stockholm University, Faculty of Science, Department of Environmental Science and Analytical Chemistry.
Stockholm University, Faculty of Science, Department of Environmental Science and Analytical Chemistry.
Number of Authors: 32019 (English)In: Analytica Chimica Acta, ISSN 0003-2670, E-ISSN 1873-4324, Vol. 1074, p. 16-32Article, review/survey (Refereed) Published
Abstract [en]

Many methods for quantifying chlorinated paraffins (CPs) yield only a total concentration of the mixture as a single value. With appropriate analytical instrumentation and quantification methods, more reliable and detailed analysis can be performed by quantifying total concentrations of short-, medium-, and longchain CPs (SCCPs, MCCPs, and LCCPs), and in the current optimal situation by quantifying individual carbon-chlorine congener groups (CnClm). Sample extraction and clean-up methods for other persistent organochlorines that have been adapted for recovery of CPs must be applied prior to quantification with appropriate quality assurance and quality control to ensure applicability of the methods for SCCPs, MCCPs, and LCCPs. Part critical review, part tutorial, and part perspective, this paper provides practical guidance to analytical chemists who are interested in establishing a method for analysis of CPs in their lab facilities using commercial reference standards, or for expanding existing analysis of total CPs or SCCPs to analysis of SCCPs, MCCPs, and LCCPs, or to analysis of CnClm congener groups.

Place, publisher, year, edition, pages
2019. Vol. 1074, p. 16-32
Keywords [en]
Short-chain chlorinated paraffins, Medium-chain chlorinated paraffins, Long-chain chlorinated paraffins, Quantification, Environmental analysis, Biomonitoring
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-170060DOI: 10.1016/j.aca.2019.02.051ISI: 000469775600002PubMedID: 31159936OAI: oai:DiVA.org:su-170060DiVA, id: diva2:1335168
Available from: 2019-07-04 Created: 2019-07-04 Last updated: 2019-07-04Bibliographically approved

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