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Chemoenzymatic Dynamic Kinetic Resolution of Primary Benzylic Amines using Pd-0-CalB CLEA as a Biohybrid Catalyst
Stockholm University, Faculty of Science, Department of Organic Chemistry. Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK). Swedish University of Agricultural Sciences, Sweden.
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Number of Authors: 102019 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 25, no 39, p. 9174-9179Article in journal (Refereed) Published
Abstract [en]

Herein, we report on the use a biohybrid catalyst consisting of palladium nanoparticles immobilized on cross-linked enzyme aggregates of lipase B of Candida antarctica (CalB CLEA) for the dynamic kinetic resolution (DKR) of benzylic amines. A set of amines were demonstrated to undergo an efficient DKR and the recyclability of the catalysts was studied. Extensive efforts to further elucidate the structure of the catalyst are presented.

Place, publisher, year, edition, pages
2019. Vol. 25, no 39, p. 9174-9179
Keywords [en]
amides, biohybrid catalysts, dynamic kinetic resolution, heterogeneous catalysis, key cross-linked enzyme aggregates
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-171741DOI: 10.1002/chem.201901418ISI: 000475680200007PubMedID: 31050831OAI: oai:DiVA.org:su-171741DiVA, id: diva2:1349465
Available from: 2019-09-09 Created: 2019-09-09 Last updated: 2019-09-09Bibliographically approved

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Yuan, NingSchreiber, Cynthia L.Tai, Cheuk-WaiZou, XiaodongBäckvall, Jan-E.
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