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Small Pore Aluminosilicate EMM-37: Synthesis and Structure Determination Using Continuous Rotation Electron Diffraction
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
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Number of Authors: 132019 (English)In: Inorganic Chemistry, ISSN 0020-1669, E-ISSN 1520-510X, Vol. 58, no 19, p. 12854-12858Article in journal (Refereed) Published
Abstract [en]

A new aluminosilicate zeolite, denoted EMM-37, with a 3D small pore channel system, has been synthesized using a diquaternary ammonium molecule as the structure directing agent (SDA) and metakaolin as the aluminum source. The structures of both as-made and calcined forms of EMM-37 were solved and refined using continuous rotation electron diffraction (cRED) data. cRED is a powerful method for the collection of 3D electron diffraction data from submicron- and nanosized crystals, which allows for successful solution and refinement of complex structures in symmetry as low as P (1) over bar.

Place, publisher, year, edition, pages
2019. Vol. 58, no 19, p. 12854-12858
National Category
Chemical Sciences
Research subject
Inorganic Chemistry
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URN: urn:nbn:se:su:diva-175814DOI: 10.1021/acs.inorgchem.9b01798ISI: 000489676400046PubMedID: 31512862OAI: oai:DiVA.org:su-175814DiVA, id: diva2:1371736
Available from: 2019-11-20 Created: 2019-11-20 Last updated: 2020-01-15Bibliographically approved
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Kapaca, ElinaWeston, Simon C.Xu, HongyiZou, XiaodongWillhammar, Tom
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