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Selective adsorption of CO2 and SF6 on mixed-linker ZIF-7-8s: The effect of linker substitution on uptake capacity and kinetics
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).ORCID iD: 0000-0002-7156-559X
Number of Authors: 42021 (English)In: Chemical Engineering Journal, ISSN 1385-8947, E-ISSN 1873-3212, Vol. 422, article id 130117Article in journal (Refereed) Published
Abstract [en]

A series of mixed-linker Zeolitic Imidazolate Framework(ZIF)-7-8s constructed from different amounts of benzimidazolate (bIm) and 2-methylimidazolate (mIm) linkers were synthesized in this study. We demonstrated that by carefully controlling the ratios between bIm and mIm linkers, the particle morphology and pore size of ZIF7-8 can be tailored to selectively adsorb CO2 or SF6 with significantly enhanced uptake capacity. ZIF-7-8 with 90% bIm and 10% mIm linkers showed a CO2 uptake of 1.44 mmol g-1 at 293 K (1 bar) and a CO2/N2 selectivity of over 30. On the other hand, ZIF-7-8 with 26% bIm and 74% mIm linkers had a high SF6 uptake of 2.08 mmol g-1 at 293 K (1 bar) as well as a high SF6/N2 selectivity of over 40. Isosteric enthalpy of adsorption calculations and cyclic adsorption experiments confirmed that both CO2 and SF6 were physisorbed on ZIF-7-8. CO2 was found to adsorb rapidly on ZIF-7-8, with over 80% of the total uptake capacity reached within 30 s. Detailed kinetics analysis concluded that the adsorption of CO2 and SF6 on these ZIF-7-8s could be described by pseudo-second order kinetics and the diffusion was found to be governed by a mixture of different mechanisms. The highly tunable sorption properties, high uptake capacity and high selectivity of ZIF-7-8 render them as interesting candidate sorbents for different greenhouse gases.

Place, publisher, year, edition, pages
2021. Vol. 422, article id 130117
Keywords [en]
Greenhouse gases, Carbon dioxide capture, Mixed-linker zeolitic imidazolate frameworks, Metal-organic frameworks
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-196848DOI: 10.1016/j.cej.2021.130117ISI: 000671784100002OAI: oai:DiVA.org:su-196848DiVA, id: diva2:1595849
Available from: 2021-09-20 Created: 2021-09-20 Last updated: 2022-02-25Bibliographically approved

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Jaworski, Aleksander

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