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Homonuclear dipolar recoupling of half-integer spin quadrupolar nuclei: techniques and applications
Stockholm University, Faculty of Science, Department of Physical, Inorganic and Structural Chemistry.
2009 (English)In: Solid State Nuclear Magnetic Resonance, ISSN 0926-2040, E-ISSN 1527-3326, Vol. 36, no 1, 1-10 p.Article in journal (Refereed) Published
Abstract [en]

We review recent advances in solid state NMR methodology for recovering homonuclear dipolar interactions among half-integer quadrupolar spins undergoing sample rotation. Existing dipolar recoupling techniques are contrasted, based on (i) the form of their associated dipolar Hamiltonian, (ii) the different experimental conditions necessitating their realization and (iii) their roles as components in multi-dimensional NMR correlation spectroscopy. Various types of structural information accessible from such solid state NMR experimentation is reviewed. Promises and limitations of methodologies targeting homonuclear dipolar couplings between half-integer spins under high-resolution conditions are discussed, with particular focus on the demands set for structural investigations of crystalline as well as structurally disordered (amorphous) inorganic network materials

Place, publisher, year, edition, pages
2009. Vol. 36, no 1, 1-10 p.
National Category
Physical Chemistry
Research subject
Materials Chemistry
URN: urn:nbn:se:su:diva-34422DOI: 10.1016/j.ssnmr.2009.06.005ISI: 000268919900001OAI: diva2:286488
Available from: 2010-01-14 Created: 2010-01-08 Last updated: 2011-07-05Bibliographically approved

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Eden, Mattias
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Department of Physical, Inorganic and Structural Chemistry
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