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Transmission electron microscopy and neutron powder diffraction studies of GdFeO3 type SrNbO3
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Moscow State University, Department of Chemistry.
Moscow State University, Department of Chemistry.
1999 (English)In: Journal of Solid State Chemistry, ISSN 0022-4596, E-ISSN 1095-726X, Vol. 147, 421-428 p.Article in journal (Refereed) Published
Abstract [en]

Stoichiometric SrNbO3; with a GdFeO3 type structure was synthesized between 1300 and 1550°C in Ar-filled and sealed niobium ampoules. Its crystal structure was refined using time-of-flight neutron diffraction data. Space group Pnma: a=√2·ap=5.6894(2) Å; b=2·ap=8.0684(1) Å; c=√2·ap=5.6944(2) Å; RF2=0.020; and RP=0.034. High-resolution electron microscopy and electron diffraction studies frequently revealed structural defects in SrNbO3. X-ray and electron diffraction studies showed cubic symmetry for SrNbO3 synthesized below 1300°C and for compounds with nominal composition Sr0.8NbO3 synthesized between 1200 and 1550°C. SrNbO3 was found to be temperature independently paramagnetic

Place, publisher, year, edition, pages
1999. Vol. 147, 421-428 p.
National Category
Materials Chemistry
Research subject
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:su:diva-43881DOI: 10.1006/jssc.1999.8357OAI: oai:DiVA.org:su-43881DiVA: diva2:371572
Available from: 2010-11-21 Created: 2010-10-29 Last updated: 2017-12-12Bibliographically approved

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