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Ruthenium-catalysed epimerisation of carbohydrate lcohols as a method to determine the equilibria for epimer interconversion in hexopyranosides
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
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2011 (English)In: European Journal of Organic Chemistry, ISSN 1434-193X, E-ISSN 1099-0690, no 23, 4455-4459 p.Article in journal (Refereed) Published
Abstract [en]

Ruthenium-catalysed epimerisation of secondary carbohydrate alcohols was used to determine the thermodynamic equilibrium between non-anomeric epimers of partially protected glucose, mannose and allose derivatives. A cyclopentadienylruthenium catalyst was used to epimerise each of two pure epimeric alcohols in two separate experiments. The epimerisation reactions were run until the same ratio of epimers was obtained from the two experiments.

Place, publisher, year, edition, pages
2011. no 23, 4455-4459 p.
Keyword [en]
Carbohydrates, ruthenium, hydrogen transfer, epimerisation
National Category
Organic Chemistry
Identifiers
URN: urn:nbn:se:su:diva-59988DOI: 10.1002/ejoc.201100504ISI: 000294347500023OAI: oai:DiVA.org:su-59988DiVA: diva2:432451
Funder
Swedish Research Council
Available from: 2011-08-03 Created: 2011-08-03 Last updated: 2017-12-08Bibliographically approved

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Träff, AnnikaBäckvall, Jan-E.
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