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Reactive consolidation of layered-ternary Ti(2)AlN ceramics by spark plasma sintering of a Ti/AlN powder mixture
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
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2011 (English)In: Journal of the European Ceramic Society, ISSN 0955-2219, E-ISSN 1873-619X, Vol. 31, no 5, 863-868 p.Article in journal (Refereed) Published
Abstract [en]

A reactive consolidation process for preparing ternary Ti(2)AlN ceramics was investigated by spark plasma sintering (SPS). A Ti/AlN powder mixture with a molar ratio of 2:1 was consolidated at temperatures ranging from 800 to 1450 degrees C. The phase composition and microstructure evolution during the process were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) equipped with an energy dispersive spectroscopy (EDS). A series of intermediate phases, namely TiN, Ti(3)Al, Ti(3)AlN and TiAl were indentified, which revealed a reaction pathway towards the formation of Ti(2)AlN.

Place, publisher, year, edition, pages
2011. Vol. 31, no 5, 863-868 p.
Keyword [en]
Powders-solid state reaction, Sintering, Hot pressing, Nitrides, Electron microscopy
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-68535DOI: 10.1016/j.jeurceramsoc.2010.11.018ISI: 000287389300026OAI: oai:DiVA.org:su-68535DiVA: diva2:472806
Note
authorCount :6Available from: 2012-01-04 Created: 2012-01-04 Last updated: 2017-12-08Bibliographically approved

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Liu, YiShen, Zhijian
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