Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
Determination of benzothiazole and benzotriazole derivates in tire and clothing textile samples by high performance liquid chromatography-electrospray ionization tandem mass spectrometry
Stockholm University, Faculty of Science, Department of Analytical Chemistry.
Stockholm University, Faculty of Science, Department of Analytical Chemistry.ORCID iD: 0000-0002-1598-7093
Stockholm University, Faculty of Science, Department of Analytical Chemistry.
Stockholm University, Faculty of Science, Department of Analytical Chemistry.
Show others and affiliations
2013 (English)In: Journal of Chromatography A, ISSN 0021-9673, E-ISSN 1873-3778, Vol. 1307, 119-125 p.Article in journal (Refereed) Published
Abstract [en]

A high performance liquid chromatography–tandem mass spectrometry method utilizing electrospray ionization in positive and negative mode has been developed for the separation and detection of benzothiazole and benzotriazole derivates. Ultra-sonication assisted solvent extraction of these compounds has also been developed and the overall method demonstrated on a selected clothing textile and an automobile tire sample. Matrix effects and extraction recoveries, as well as linearity and limits of detection have been evaluated. The calibration curves spanned over more than two orders of magnitude with coefficients of correlation R2 > 0.99 and the limits of detection and the limits of quantification were in the range 1.7–58 pg injected and 18–140 pg/g, respectively. The extraction recoveries ranged between 69% and 102% and the matrix effects between 75% and 101%. Benzothiazole and benzotriazole derivates were determined in the textile sample and benzothiazole derivatives determined in the tire sample with good analytical performance.

Place, publisher, year, edition, pages
2013. Vol. 1307, 119-125 p.
Keyword [en]
HPLC–MS/MS, Benzothiazoles, Benzotriazoles, Automobile tire, Textile sample
National Category
Analytical Chemistry
Identifiers
URN: urn:nbn:se:su:diva-93450DOI: 10.1016/j.chroma.2013.07.087ISI: 000324005500015OAI: oai:DiVA.org:su-93450DiVA: diva2:646948
Available from: 2013-07-26 Created: 2013-09-10 Last updated: 2017-11-10Bibliographically approved

Open Access in DiVA

No full text

Other links

Publisher's full text

Search in DiVA

By author/editor
Avagyan, RozannaSadiktsis, IoannisThorsen, GunnarÖstman, ConnyWesterholm, Roger
By organisation
Department of Analytical Chemistry
In the same journal
Journal of Chromatography A
Analytical Chemistry

Search outside of DiVA

GoogleGoogle Scholar

doi
urn-nbn

Altmetric score

doi
urn-nbn
Total: 54 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf