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Single-Crystal Structure of a Covalent Organic Framework
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
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2013 (English)In: Journal of the American Chemical Society, ISSN 0002-7863, E-ISSN 1520-5126, Vol. 135, no 44, 16336-16339 p.Article in journal (Refereed) Published
Abstract [en]

The crystal structure of a new covalent organic framework, termed COF-320, is determined by single-crystal 3D electron diffraction using the rotation electron diffraction (RED) method for data collection. The COF crystals are prepared by an imine condensation of tetra-(4-anilyl)methane and 4,4'-biphenyldialdehyde in 1,4-dioxane at 120 degrees C to produce a highly porous 9-fold interwoven diamond net. COF-320 exhibits permanent porosity with a Langmuir surface area of 2400 m(2)/g and a methane total uptake of 15.0 wt % (176 cm(3)/cm(3)) at 25 degrees C and 80 bar. The successful determination of the structure of COF-320 directly from single-crystal samples is an important advance in the development of COF chemistry.

Place, publisher, year, edition, pages
2013. Vol. 135, no 44, 16336-16339 p.
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-97382DOI: 10.1021/ja409033pISI: 000326774300024OAI: oai:DiVA.org:su-97382DiVA: diva2:678207
Funder
Knut and Alice Wallenberg FoundationVinnova
Note

AuthorCount:8;

Available from: 2013-12-11 Created: 2013-12-09 Last updated: 2017-12-06Bibliographically approved

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