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The First One-Pot Synthesis of Metal-Organic Frameworks Functionalised with Two Transition-Metal Complexes
Stockholm University, Faculty of Science, Department of Organic Chemistry. Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
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2015 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 21, no 2, 861-866 p.Article in journal (Refereed) Published
Abstract [en]

The synthesis of a metal-organic framework (UiO-67) functionalised simultaneously with two different transition metal complexes (Ir and Pd or Rh) through a one-pot procedure is reported for the first time. This has been achieved by an iterative modification of the synthesis parameters combined with characterisation of the resulting materials using different techniques, including X-ray absorption spectroscopy (XAS). The method also allows the first synthesis of UiO-67 with a very wide range of loadings (from 4 to 43 mol%) of an iridium complex ([IrCp*(bpydc)(Cl)Cl](2-); bpydc=2,2'-bipyridine-5,5'-dicarboxylate, Cp* = pentamethylcyclopentadienyl) through a pre-functionalisation methodology.

Place, publisher, year, edition, pages
Wiley-VCH Verlagsgesellschaft, 2015. Vol. 21, no 2, 861-866 p.
Keyword [en]
functionalisation, metal-organic frameworks, microporous materials, synthesis design, transition metal complexes
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-113542DOI: 10.1002/chem.201403909ISI: 000347231300042OAI: oai:DiVA.org:su-113542DiVA: diva2:787088
Funder
Knut and Alice Wallenberg FoundationSwedish Research CouncilVINNOVA
Note

AuthorCount:5;

Available from: 2015-02-09 Created: 2015-02-04 Last updated: 2017-11-09Bibliographically approved

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Platero-Prats, Ana E.Bermejo Gómez, AntonioZou, Xiaodong
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