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  • 1. Pouchly, V.
    et al.
    Maca, K.
    Xiong, Yan
    Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
    Shen, J. Zhijian
    Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
    Master Sintering Surface: A practical approach to its construction and utilization for Spark Plasma Sintering prediction2012In: Science of Sintering, ISSN 0350-820X, Vol. 44, no 2, p. 169-175Article in journal (Refereed)
    Abstract [en]

    The sintering is a complex thermally activated process, thus any prediction of sintering behaviour is very welcome not only for industrial purposes. Presented paper shows the possibility of densification prediction based on concept of Master Sintering Surface (MSS) for pressure assisted Spark Plasma Sintering (SPS). User friendly software for evaluation of the MSS is presented. The concept was used for densification prediction of alumina ceramics sintered by SPS.

  • 2. Wang, Ling
    et al.
    Pouchly, Vaclav
    Maca, Karel
    Shen, Zhijian
    Stockholm University, Faculty of Science, Department of Materials and Environmental Chemistry (MMK).
    Xiong, Yan
    Intensive particle rearrangement in the early stage of spark plasma sintering process2015In: Journal of Asian ceramic societies, ISSN 2187-0764, Vol. 3, no 2, p. 183-187Article in journal (Refereed)
    Abstract [en]

    The densification behaviors of 3 mol% yttria-stabilized tetragonal zirconia polycrystal (3Y-TZP) ceramics during spark plasma sintering (SPS) were analyzed both using the master sintering curve (MSC) approach and by evaluating the temperature dependent evolution of density and densification rate. It was found that densification curves could hardly be fitted using one apparent activation energy value by MSC conception, by which it indicated that more than one densification mechanisms were involved in SPS. Moreover, dependent neither on applied pressure (20-100 MPa) nor heating rates higher than 50 degrees C/min, the maximum densification rate had always been observed at rather similar similar to 78% of theoretical density (TD) accompanied with negligible grain growth. An intensive particle rearrangement mechanism was proposed to dominate the rapid densification to 78% TD in early stage of SPS process, by which it yielded the considerable faster densification rate than those achievable by diffusion-related processes. (C) 2015 The Ceramic Society of Japan and the Korean Ceramic Society.

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