Lundberg, Helena (0000-0002-4704-1892)

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Lundberg, Helena ORCID iD icon

orcid.org/0000-0002-4704-1892

Publications (1 of 1) Show all publications

Lundberg, H., Tinnis, F. & Adolfsson, H. (2019). Zirconium catalyzed amide formation without water scavenging. Applied organometallic chemistry, 33(9), Article ID e5062.

Open this publication in new window or tab >>Zirconium catalyzed amide formation without water scavenging

Lundberg, Helena

Tinnis, Fredrik

Adolfsson, Hans

2019 (English)In: Applied organometallic chemistry, ISSN 0268-2605, E-ISSN 1099-0739, Vol. 33, no 9, article id e5062Article in journal (Refereed) Published

Abstract [en]

A scalable homogeneous metal-catalyzed protocol for direct amidation of carboxylic acids is presented. The use of 2-10 mol% of the commercially available Zr(Cp)(2)(OTf)(2)center dot THF results in high yields of amides at moderate temperature, using an operationally convenient reaction protocol that circumvents the use of water scavenging techniques.