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Ruthenium-Catalyzed Aminocarbonylation with Isocyanates Through Weak Coordinating Groups
Stockholm University, Faculty of Science, Department of Organic Chemistry. AstraZeneca, Sweden.ORCID iD: 0000-0002-0904-2835
Number of Authors: 42023 (English)In: Chemistry - A European Journal, ISSN 0947-6539, E-ISSN 1521-3765, Vol. 29, no 61, article id e202302023Article in journal (Refereed) Published
Abstract [en]

Introducing amide functional groups under mild conditions has growing importance owing to the prevalence of such moiety in biologically active molecules. Herein, we disclose a mild protocol for the directed ruthenium-catalyzed C−H aminocarbonylation with isocyanates as the amidating agents developed through high-throughput experimentation (HTE). The redox-neutral and base-free reaction is guided by weakly Lewis basic functional groups, including anilides, lactams and carbamates to access anthranilamide derivatives. The synthetic utility of this transformation is reflected by large-scale synthesis and late-stage functionalization.

Place, publisher, year, edition, pages
2023. Vol. 29, no 61, article id e202302023
Keywords [en]
amidations, C-H activation, density functional calculations, high-throughput experimentation, ruthenium
National Category
Organic Chemistry
Identifiers
URN: urn:nbn:se:su:diva-223948DOI: 10.1002/chem.202302023ISI: 001068158400001PubMedID: 37737512Scopus ID: 2-s2.0-85171783447OAI: oai:DiVA.org:su-223948DiVA, id: diva2:1814711
Available from: 2023-11-27 Created: 2023-11-27 Last updated: 2024-01-15Bibliographically approved

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Johansson, Magnus J.

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